【摘要】 在一定的压力下 ,以甲基三甲氧硅烷 ,氯代环己烷和镁为原料通过格氏法合成甲基环己基二甲氧基硅烷。考察了溶剂、原料配比、反应温度、时间和压力等因素对产率的影响。在适宜的反应条件下 ,甲基环己基二甲氧基硅烷的产率可达 90 5 %。更多还原

【Abstract】 At a pressure,methylcyclohexyldimethoxysilane is prepared by reaction of methyltrimethoxysilane with cyclohexyl chloride Grignard reagents in a pot.Factors of influence such as solvent type and amount, molar ratio of raw materials, reaction temperature, time and pressure are investigated.In suitable conditions,yield of the title compound can reach 90 5%.更多还原