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新型钻井液甲基葡萄糖苷的合成研究
Synthesis of New Typeof Methyl Glucoside Drilling Fluild System
【摘要】 研究了催化剂、反应温度、反应时间、配料比、后处理等因素对甲基葡萄糖苷合成反应过程及结果的影响 ,得出了适宜反应条件 ,反应温度为70℃ ,甲醇∶葡萄糖∶催化剂=8∶1∶0.02(摩尔比) ,反应时间为8h。产品收率(DP=1.64)为86 %。
【Abstract】 It was studied that the influencing factors of catalyst?reaction temperature and time?mole ratio of raw material?product treatment etc.to methyl glucoside synthesis process.The suitable conditions for the reaction were obtained,reaction temperature 70℃,n(methnol)∶n(glucose)∶n(catalyst)=8∶1∶0.02,reaction time 8 hours,yield of the product (degree of polymerization was 1.64) was 86%.
- 【文献出处】 河北化工 ,Heibei Chemical Engineering and Industry , 编辑部邮箱 ,2002年06期
- 【分类号】TE254
- 【被引频次】8
- 【下载频次】372