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顺丁烯二酸二异辛酯制备工艺改进

An improved synthesis of 2-Ethylhexyl Maleate

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【作者】 王文涛文福姬李健秀王琨

【Author】 Wang Wentao Li Jianxiu Wen Fuji Wang Kun (Dept·of Pharmacy and Applied Chemistry,Jilin Institute of Chemical Technolo gy, Jilin City 132022)

【机构】 吉林化工学院制药与应用化学系吉林化工学院制药与应用化学系 132022132022132022

【摘要】 以离子交换树脂作催化剂制备了顺丁烯二酸二异辛酯,同时与硫酸、对甲苯磺酸催化工艺进行了比较。并应用正交实验得到了最佳反应条件,此条件下目的产物收率为97.64%。离子交换树脂作催化剂与产品容易分离,后处理工艺简单,且减少废水排放。

【Abstract】 An improved method using exchange resin catalyst ion for the prepara ti on of title compound was described in this paper. At the same time,the methods u sing sulfuric acid and so on as catalysts were compared.And the optimimum reacti on conditions were obtaine.Under this condition,the yield was 97.36%.The new p rocess was not only simple but can reduce drain wastewater. And the catalysts we re separated easily from the reactant.

  • 【文献出处】 安徽化工 ,Anhui Chemical Industry , 编辑部邮箱 ,2002年06期
  • 【分类号】TQ225.24
  • 【被引频次】1
  • 【下载频次】93
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