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尿素包合法纯化α-亚麻酸工艺研究(Ⅰ)——α-亚麻酸纯化过程单因素实验研究

Purity Method of α-Linolenic Acid Based on the Theory of Urea Adduction Fractionation(Ⅰ) ——Study on the Noticeable Factors Affecting Purification Behavior of α-Linolenic Acid

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【作者】 张海满刘福祯戴玲妹

【Author】 ZHANG Hai man,LIU Fu zhen,DAI Ling mei (Department of Chemical Engineering,Tsinghua University,Beijing,China)

【机构】 清华大学化学工程系!100084北京市

【摘要】 利用尿素包合原理主要分析了通过尿素包合分离、提纯α 亚麻酸的过程中包合温度、尿素用量、溶剂配比、包合时间和包合次数等主要操作条件对产品α 亚麻酸的纯度、收率的影响。使α 亚麻酸的浓度由 4 6 7%提高到 87 3% ,收率 53 5%

【Abstract】 The α linolenic acid with high purity is purified with Urea adduction fractionation method from the fatty acids mixture which is produced by linseed oil saponification.The paper discussed the factors in detail,such as operation temperature,adduction time and the feed ratio of Urea and MeOH to fatty acids,witch effect the α linolenic acid purity and yield remarkably,based on the theory of Urea adduction fractionation.The purity of α linolenic acid is increased from 46 7%to87 3%.The yield of α linolenic acid is about 53 5%.

【关键词】 亚麻油α亚麻酸尿素包合提纯
【Key words】 Linseed oilα Linolenic acidUrea fractionationpurification
  • 【文献出处】 中国油脂 ,China Oils and Fats , 编辑部邮箱 ,2001年02期
  • 【分类号】TQ644
  • 【被引频次】99
  • 【下载频次】749
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