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J酸清洁生产新工艺的研究
Research on new technology of J acid clean production.
【摘要】 借助高压液相色谱研究了J酸清洁生产新工艺,优化了J酸制备的反应条件,按照新工艺,产品的干品含量(偶合值)高于95%,而杂质异构体γ酸含量低于0.5%,J酸对吐氏酸的总收率达76%,减少了废水的排放.
【Abstract】 A new technology of J acid clean production was studied to optimize the reaction conditions for preparation of J acid by means of HPLC. With this new method, the content (coupling value) of dried product is higher then 95%, and the content of isomer γacid impurity is less then 0.5%, total yield of J acid based on Tobias acid is 76 percent, and wastewater discharge can be decreased.
【关键词】 J酸;
清洁生产;
磺化;
碱熔;
高压液相色谱;
【Key words】 J acid; clean production; sulfonation; caustic fusion; HPLC;
【Key words】 J acid; clean production; sulfonation; caustic fusion; HPLC;
- 【文献出处】 中国环境科学 ,China Environmental Science , 编辑部邮箱 ,2001年05期
- 【分类号】X383
- 【被引频次】2
- 【下载频次】299