节点文献
对羟基苯甲酸苄酯的合成
Synthesis of Benzyl p-hydroxybenzoate
【Abstract】 Benzyl p hydroxybenzoate was prepared from benzyl chloride and p hydroxybenzoic acid by phase transfer catalysis, in which xylene was used as an organic solvent, Na 2CO 3 aqueous solution as a condensing agent and Bu 4NCl as a phase transfer catalyst. The effects of reaction time, Na 2CO 3 concentration and feed amount of raw materials were investigated. The concentration of Na 2CO 3 aqueous solution was the most important factor. Prodact with purity greater 98% and yield more 85% was obtained.
【基金】 辽宁省优秀青年科技人才培养基金!( 973 0 0 7);大连理工大学精细化工国家重点实验室资助项目
- 【文献出处】 应用化学 ,Chinese Journal of Applied Chemistry , 编辑部邮箱 ,2001年04期
- 【分类号】TQ24
- 【被引频次】25
- 【下载频次】277