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火焰原子光谱法直接测定可溶性有机物中微量元素

Direct determination of micro elem ents in dissoluble organic matter by flame atomic spectrometry

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【作者】 张起凯刘立行赵志芬

【Author】 ZHANG Qi kai,LIU Li xing, ZHAO Zhi fen (Department of Applied Chemistry,F ushun Petroleum Institute,Fushun 1 13001,China)

【机构】 抚顺石油学院应用化学系抚顺石油学院应用化学系 辽宁抚顺113001辽宁抚顺113001辽宁抚顺113001

【摘要】 建立了用火焰原子光谱法测定中药冲剂中钾、镁的快速分析方法。用硝酸溶液 (1+ 1)溶解样品 ,分别以吸收法及发射法测定镁、钾。工作曲线法的测定结果与灰化法一致 ,相对误差小于± 0 8% ,t检验表明本方法与灰化法之间无显著性差异。方法简便、快速、准确

【Abstract】 An analytical method for r apid determination of potassium an d magnesium in electuary of tradi tional Chinese medicine(ETCM)by fl ame atomic spectrometry has been d eveloped Sample was dissolved by nitric acid(1+1) FAAS and FAES wer e used to determine magnesium and potassium,respectively Determinati on results of the working curve me thod were consistent with those ob tained by ashing method The relati ve error between them was less tha n ±0 8% The t test showed that no difference was found between two m ethods This method is convenient,r apid and accurate

  • 【文献出处】 冶金分析 ,Metallurgical Analysis , 编辑部邮箱 ,2001年06期
  • 【分类号】O657.31
  • 【下载频次】97
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