节点文献
乳酸精制新工艺——刮膜蒸发和短程蒸馏联用法
A new refining process for lactic acid by combined wiped film vaporization and short term distillation
【摘要】 2 0 %~ 30 %粗乳酸经刮膜蒸发器 ,在 1 0 0 0~ 70 0 0Pa,60~ 1 0 0℃条件下蒸发 5~ 2 5min ,得到 80 %~ 90 %亚纯乳酸。亚纯乳酸再经短程蒸馏器 ,在 1 0~ 1 0 0Pa ,60~ 90℃条件下蒸馏 0 .5~ 5min得到纯乳酸。这种方法不用活性炭脱色和离子交换 ,仅经过两次减压蒸馏就能得到达到国家标准的纯乳酸。
【Abstract】 A new process for refining lactic acid was suggested.The sub pure lactic acid (80%~90%) was obtained by vaporization of the raw lactic acid (20%~30%) at 1 000~7 000 Pa and 60~100℃ in wiped film vaporizer for 5~25 minutes.The pure lactic acid could be obtained by distillation at 10~100 Pa and at 60~90℃ for 0 5~5 minutes.Without using active carbon for decolorization and ion exchange technique,the new process could produce pure lactic acid meeting the specifications of national standard only by vacuum distillation twice.
【Key words】 lactic acid; refining; wiped film vaporization; short term distillation;
- 【文献出处】 现代化工 ,Modern Chemical Industry , 编辑部邮箱 ,2001年01期
- 【分类号】TQ225.41;TQ02
- 【被引频次】22
- 【下载频次】302