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乳酸精制新工艺——刮膜蒸发和短程蒸馏联用法

A new refining process for lactic acid by combined wiped film vaporization and short term distillation

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【作者】 吕九琢徐亚贤袁光韩锡广

【Author】 LU Jiu zhuo 1, XU Ya xian 1, YUAN Guang 1, HAN Xi guang 2 (1. Department of Chemical Engineering, Beijing Institute of Petro Chemical Technology, Beijing 102600, China; 2.Kazuo Organic Acid Company of Liaoning Province, Kezhou County 122300, Ch

【机构】 北京石油化工学院化工系!北京102600辽宁喀左县有机酸公司!喀左县122300

【摘要】 2 0 %~ 30 %粗乳酸经刮膜蒸发器 ,在 1 0 0 0~ 70 0 0Pa,60~ 1 0 0℃条件下蒸发 5~ 2 5min ,得到 80 %~ 90 %亚纯乳酸。亚纯乳酸再经短程蒸馏器 ,在 1 0~ 1 0 0Pa ,60~ 90℃条件下蒸馏 0 .5~ 5min得到纯乳酸。这种方法不用活性炭脱色和离子交换 ,仅经过两次减压蒸馏就能得到达到国家标准的纯乳酸。

【Abstract】 A new process for refining lactic acid was suggested.The sub pure lactic acid (80%~90%) was obtained by vaporization of the raw lactic acid (20%~30%) at 1 000~7 000 Pa and 60~100℃ in wiped film vaporizer for 5~25 minutes.The pure lactic acid could be obtained by distillation at 10~100 Pa and at 60~90℃ for 0 5~5 minutes.Without using active carbon for decolorization and ion exchange technique,the new process could produce pure lactic acid meeting the specifications of national standard only by vacuum distillation twice.

  • 【文献出处】 现代化工 ,Modern Chemical Industry , 编辑部邮箱 ,2001年01期
  • 【分类号】TQ225.41;TQ02
  • 【被引频次】22
  • 【下载频次】302
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