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杜仲叶中桃叶珊瑚甙测定方法的研究

Study on Measuring Method of Aucubin in Eucommia ulmoids Leaf

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【作者】 董娟娥马柏林贾二红

【Author】 DONG Juan e 1, MA Bai lin 2, JIA Er hong 1 (1.College of Forestry, NW Sci Tech Uni. of Agr. and For.,Yangling , Shaanxi 712100, China; 2.College of Life Sciences,NW Sci Tech Uni. of Agr. and For.,Yangling , Shaanxi 712100, China)

【机构】 西北农林科技大学林学院!陕西杨陵712100西北农林科技大学生命科学学院

【摘要】 对文献 [4,5,6]中介绍的实验室桃叶珊瑚甙测定方法进行了分析比较 ,结果认为“对二甲氨基苯甲醛法”简便易行 ,但却存在着测定液中出现聚沉现象 ,且所测含量偏大 ,因为该方法不能将植物体中共存的京尼平甙和京尼平甙酸分离 ,测定结果为桃叶珊瑚甙与这些同类环烯醚萜类化合物的含量之和。为此 ,研究出“改进对二甲氨基苯甲醛法” ,用该方法测定桃叶珊瑚甙简便易行 ,测定数值较为精确。

【Abstract】 Three laboratory determining methods introduced in documents on aucubin were analysed. The result of comparison showed that the Epstahl method could be feasible. However, there remained an issue that precipitate occurred in determining solution, and the determined content was inclined to be beyond the real level, because this method was not effective in separating geniposide and geniposide acid from coexisting iridoids in E.ulmoids the content is the sum. By determining and analysis, improved epstahl method is advocated to solve the mentioned issue, which is proved to be simple, feasible and reliable.

【基金】 陕西省重大科技项目!(97K0 4- G2 )
  • 【文献出处】 西北林学院学报 ,Journal of Northwest Forestry College , 编辑部邮箱 ,2001年01期
  • 【分类号】Q946.8
  • 【被引频次】76
  • 【下载频次】394
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