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多级喷雾碳化法制备纳米碳酸钙工艺研究
Preparation of Nanometer Calcium Carbonate by Multistage Spray Carbonation
【摘要】 研究了多级喷雾碳化法制备纳米碳酸钙的工艺,并详细讨论了雾化、碳化条件及添加剂量等对纳米碳酸钙粒径的影响.碳化后的沉淀物经真空干燥,其原始粒径约为30nm.经表面改性处理,可得到粒径在30~40nm范围的活性纳米碳酸钙粉体材料.
【Abstract】 The preparation process of nanometer calcium carbonate(CaCO3) by multistage spray carbonation was studied. The effects of the conditions of spray carbonation and additive dosage on the average particle size of nanometer CaCO3 were discussed systematically. The primary particle size of carbonated sediment was about 30nm by vacuum desiccation. Then the active nanometer CaCO3 particles ranged from 30nm to 40nm were obtained by means of surfaction.
【关键词】 纳米碳酸钙;
喷雾碳化;
粒径;
传质系数;
【Key words】 nanometer calcium carbonate; multistage spray carbonation; particle size; mass transfer coefficient;
【Key words】 nanometer calcium carbonate; multistage spray carbonation; particle size; mass transfer coefficient;
- 【文献出处】 无机材料学报 ,Journal of Inorganic Materials , 编辑部邮箱 ,2001年05期
- 【分类号】TB383
- 【被引频次】31
- 【下载频次】248