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养血生发胶囊中何首乌羟芪衍生物的含量测定

Determination of Hydroxystilbene Glucopyranoside of Radix Polygoni multiflori in Yangxueshengfa Capsules by RP-HPLC

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【作者】 蒋琴鞠建明鲁静

【Author】 JIANG Qin 1, JU Jian ming 2, LU Jing 3 (1.Nanjing Hospital of Traditional Chinese Medicine, 210001, China; 2.Jiangsu Academy of Traditional Chinese Medicine, Nanjing 210028, China; 3.China Institute for the Control of Pharmaceutical and Biological

【机构】 江苏省南京市中医院!210001江苏省中医药研究院!江苏南京210028中国药品生物制品检定所!北京100050

【摘要】 目的 :测定养血生发胶囊中何首乌含有的 2 ,3 ,5 ,4’—四羟基二苯乙烯 -2 -0 -β-D-葡萄糖苷的含量。方法 :采用反相高效液相色谱 (RP-HPL C)法。流动相为乙腈 -水 (2 0∶ 80 ) ,流速 1.0 ml/ min,检测波长 3 2 0 nm。结果 :回收率为 97.2 1% ,RSD为1.83 % (n=6)。结论 :方法简便、可靠、易行

【Abstract】 Objective:To determine 2,3,5,4’ tetrahydroxystilbene 2 0 β D glucopyranoside in Radix Polygoni multiflori in Yangxueshengfa Capsules.Methods:RP-HPLC was used in the quantitative analysis using acetonitrile∶water (20∶80) as mobile phase. The flow rate was 1.0 ml/min and detect wave was 320 nm.Results:The recovery was 97.21% and RSD (%) was 1.83 ( n =6).Conclusion:This RP-HPLC method is simple,reliable and easy to apply.

  • 【文献出处】 时珍国医国药 ,LiShiZhen Medicine and Materia Medica Research , 编辑部邮箱 ,2001年09期
  • 【分类号】R284.2
  • 【被引频次】16
  • 【下载频次】153
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