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氨基磺酸法合成AESA研究

The studies of synthesiaing AESA With Sulfamic Acid

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【作者】 姚志钢谢佐才戴云信

【Author】 YAO Zhi_gang XIE Zuo_cai DAI Yun_xi (Department of Chemical Engineering,Shaoyang College,Shaoy Hunan,422001)

【机构】 邵阳高等专科学校化学工程系邵阳高等专科学校化学工程系 湖南邵阳422001湖南邵阳422001湖南邵阳422001

【摘要】 介绍了氨基磺酸化为硫酸作剂的优点 ,详细讨论了各种因素对合成AESA的影响 ,得出了最佳工艺条件 :摩尔配比NH2 SO3 H∶AEO3 =1∶1.0 5 ,反应温度 115~ 12 0℃ ,反应时间 12 0~ 15 0min ,催化剂用量为 1% ,助催化剂用量为 6 % .

【Abstract】 The advantages of sulfamic acid as a kind of sulfating agent were emphasized in this paper,The factors affecting synthesis of AESA were in detail studied,and the optimum conditions were obtained: the molar ration of sulfamic acid to AEO 3 was 1∶1.05,the reaction temperature was 115~120℃,the reaction time was 120~150min .the dosage of catalysis was 1%,the dosage of aid catalysis was 6% .

【关键词】 氨基磺酸AESA醇醚硫酸铵硫酸酯化
【Key words】 Sulfamic AcidAESAwmmonium laureth sulfatsulfating
  • 【文献出处】 邵阳高等专科学校学报 ,Journal of Shaoyang College , 编辑部邮箱 ,2001年03期
  • 【分类号】TQ423
  • 【被引频次】16
  • 【下载频次】245
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