节点文献
氨基磺酸法合成AESA研究
The studies of synthesiaing AESA With Sulfamic Acid
【摘要】 介绍了氨基磺酸化为硫酸作剂的优点 ,详细讨论了各种因素对合成AESA的影响 ,得出了最佳工艺条件 :摩尔配比NH2 SO3 H∶AEO3 =1∶1.0 5 ,反应温度 115~ 12 0℃ ,反应时间 12 0~ 15 0min ,催化剂用量为 1% ,助催化剂用量为 6 % .
【Abstract】 The advantages of sulfamic acid as a kind of sulfating agent were emphasized in this paper,The factors affecting synthesis of AESA were in detail studied,and the optimum conditions were obtained: the molar ration of sulfamic acid to AEO 3 was 1∶1.05,the reaction temperature was 115~120℃,the reaction time was 120~150min .the dosage of catalysis was 1%,the dosage of aid catalysis was 6% .
- 【文献出处】 邵阳高等专科学校学报 ,Journal of Shaoyang College , 编辑部邮箱 ,2001年03期
- 【分类号】TQ423
- 【被引频次】16
- 【下载频次】245