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表面活性剂对制备纳米MoS2颗粒的影响

INFLUENCE OF SURFACTANTS ON THE PREPARATION OF MoS2 NANOPARTICLES

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【作者】 曾颖峰; 蒋晓明; 陈月珠;

【Author】 ZENG Ying feng,JIANG Xiao ming,CHEN Yue zhu (State Key Laboratory of Heavy Oil Processing,University of Petroleum,Beijing 102200,China)

【机构】 石油大学重质油加工国家重点实验室!北京102200;

【摘要】 采用沉淀法制备 Mo S2 纳米颗粒 ,考察了不同类型的表面活性剂对生成 Mo S2 颗粒的影响。用透射电子显微镜 ( TEM)考察了几种表面活性剂对颗粒形貌的影响 ;用红外光谱 ( IR)考察了改性后的纳米颗粒的表面结构。结果表明 ,阳离子型表面活性剂对 Mo S2 纳米颗粒的改性效果最好 ,十六烷基三甲基氯化铵改性的 Mo S2 纳米颗粒的粒径在 1 0 0 nm左右 ,且具有亲油疏水性

【Abstract】 Molybdenum disulfide (MoS 2) nanoparticles were prepared by precipitation method at the presence of different surfactants, such as dialkyldithiophosphate (DDP), cetyl trimethyl ammonium chloride and polyvinyl alcohol (PVA). The influence of surfactants on the size and appearance of prepared MoS 2 nanoparticles was investigated. The morphology and structure of these prepared particles were characterized by means of TEM and IR, etc.. The results showed that MoS 2 nanoparticles modified by cetyl trimethyl ammonium chloride were uniform, their diameter were around 100 nm, and showed some lipophilic characteristics.

  • 【文献出处】 石油学报(石油加工) ,Acta Petrolei Sinica (Petroleum Processing Section) , 编辑部邮箱 ,2001年04期
  • 【分类号】O614.61
  • 【被引频次】67
  • 【下载频次】541
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