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微波消解ICP-AES法测定茶叶中铅、砷、铜、铁、锌、硒等12种元素的含量

Determination of Arsenic,Lead,Iron,Copper,Selenium all Together 12 Elements in Tea by ICP-AES with Microwave Clear up System

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【摘要】 研究了用微波消解前处理样品,ICP-AES法同时测定茶叶中铅、砷、铜、镉、锰、铁、锌、硒等12个元素含量的方法,并对样品前处理、酸度及茶叶中共存元素干扰的影响等因素进行了探讨,该方法的回收率在84.5%~115%之间,精密度RSD均小于9%,该方法能满足茶叶测定要求。

【Abstract】 Tea was digested by MDS- 2000 microwave clear up system,Arsenic,lead,Iron,Copper,Selenium all together 12 elements were determined. This paper study the method of dealing with the tea sample and determination conditions by ICP- AES,Influence such as acidity elements interferenence were discussed.The rate of recovery of the 12 elements is from 84.5% to 1.5% ,and the relation standard deviation (RSD)is less than 9.0% ,The results was satisfactory for tea.

  • 【分类号】TS272.7
  • 【被引频次】57
  • 【下载频次】720
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