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强酸性阳离子交换树脂催化合成乳酸正丁酯
Catalytic Synthesis of N- Butyl Lactate by Strongly Acidic Cationic Exchange Resin
【摘要】 在强酸性阳离子交换树脂存在下,由乳酸和正丁醇合成了乳酸正丁酯。当乳酸和正丁醇的摩尔比为 1∶ 2,强酸性阳离子交换树脂的用量 0. 5 g,回流分水 100 min时酯收率达 99. 3%。同时,研究了催化剂的重复使用性能。
【Abstract】 N- butyl lactate was synthesized from lactic acid and n- butyl alcohol in the presence of strongly acidic cationic exchange resin. The yield of the ester can reach 99.3% under mole ratio of lactic acid and n- butyl alcohol was 0.1:0.2, the amount of strongly acidic cationic exchange resin was 0.5 g, refluxing and water seprating for 100 min. The reusability of the catalyst was studied.
【关键词】 乳酸正丁酯;
合成;
强酸性阳离子交换树脂;
催化剂;
【Key words】 n- butyl lactate; synthesis; strongly acidic cationic exchange resin; catalyst;
【Key words】 n- butyl lactate; synthesis; strongly acidic cationic exchange resin; catalyst;
- 【文献出处】 化工生产与技术 ,Chemical Production and Technology , 编辑部邮箱 ,2001年02期
- 【分类号】TQ413
- 【被引频次】14
- 【下载频次】89