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锆-铝复合氧化物的制备及酸腐蚀对其表面性质的影响
Preparation and Evaluation of Acid-Corroded Zirconia-Alumina Composites as HPLC Support
【摘要】 利用溶胶 -凝胶技术制备了 Zr O2 - Al2 O3复合氧化物。考察了不同的投料比时复合氧化物的物理化学性质 ,比较了不同浓度酸腐蚀前后氧化物微球的比表面积、孔径、表面酸碱性及复合氧化物中氧化锆、氧化铝摩尔比等物理化学参数的变化
【Abstract】 A new support, zirconia alumina spherical particles, was synthesized by means of a sol gel method. The physicochemical properties such as the acid base properties, the pore volume, the surface area and the average pore diameter of this novel support before and after acid treatment were investigated. The results show that the acid corroded zirconia alumina support is of a larger surface area and better pore structure as compared with the native zirconia alumina particles.
【关键词】 ZrO2-Al2O3复合氧化物;
酸腐蚀;
色谱填料;
【Key words】 Zirconia alumina composites; Acid corrosion; Stationary phase for HPLC;
【Key words】 Zirconia alumina composites; Acid corrosion; Stationary phase for HPLC;
【基金】 国家自然科学基金 (No.2 9875 0 2 0 )
- 【文献出处】 分析科学学报 ,Journal of Analytical Science , 编辑部邮箱 ,2001年05期
- 【分类号】O614
- 【被引频次】5
- 【下载频次】135