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高效液相色谱法测定20%增效噻枯唑可溶性粉剂中噻枯唑含量
Quantitative Determination of 20% MBAMT Wettable Powders by High Performance Liquid Chromatograph
【摘要】 建立了 2 0 %增效可溶性噻枯唑 ( MBAMT)粉剂中有效成分 MBAMT的高效液相色谱 ( HPLC)分析方法。采用硅胶柱 ,正已烷∶无水乙醇 =9∶ 2 ( V/V )为流动相 ,所得结果良好 ,平均回收率为 93.75 % ,变异系数为 2 .1 8%。方法简易、快速、准确 ,已用于产品质检
【Abstract】 The HPLC method for determination of MBAMT(N,N′ methylene bis(2 amino 5 mercapto 1,3,4 thiadia zole)has been reported. The sample was analyzed on a SiO 2 column with mobile phase of n hexane∶ethyl alcohol=9∶2( V/V )using UV detector at 320 nm. The variation coefficient, recovery were 2.183% and 93.76%, respectively. The analytical results show that this method is simple, rapid and accurate.
- 【文献出处】 分析科学学报 ,Journal of Analytical Science , 编辑部邮箱 ,2001年02期
- 【分类号】O657.72
- 【被引频次】3
- 【下载频次】62