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2-羟基-3-(二甲基十二烷基铵)丙磺酸钠合成和性能测试
Synthesis and Properties of Sodium 2-Hydroxy-3- (Dimethyl Dodecyl Ammonium) Propyl Sulphonate
【摘要】 2 -羟基 -3 -(二甲基十二烷基铵 )丙磺酸钠 (Ⅰ )是由二甲基十二烷基胺 (Ⅱ )与 2 -羟基 -3 -氯丙磺酸钠(Ⅲ )合成。反应最佳条件 :温度 90℃ ,时间 4h ,溶剂丙三醇 ,化合物 (Ⅱ )转化率达 90 %。实验结果表明 ,化合物 (Ⅰ )具有比甜菜碱BS -12更优良的润湿力、泡沫力和泡沫稳定性 ,还具有比十二烷基硫酸钠更优良的钙皂分散力
【Abstract】 The titlle compound sodium 2-hydroxy-3-(dimethyl dodecyl ammonium)proply sulphonate(Ⅰ)is a kind of the amphoteric surfactant.The title compound(Ⅰ)was synthesized from dimethyldodecylamine(Ⅱ)and sodium 2-hydroxy-3-chloropropyl sulphonate(Ⅲ).The best condition for the reaction(temperature 90 ℃,time 4h,solvent glycerol.)were chosenby the orthogonal design.The inversion rate of(Ⅱ)was 90 %.The test resultshowed that(Ⅰ)had better wetting,forming and foam stability than betaine BS-12,and better dispersion of calcium soap than dodecyl sulfate sodium.
【Key words】 amphoteric surfactant; sulfobetaine; wetting agent; dispersion of calcium soap;
- 【文献出处】 日用化学工业 ,China Surfactant Detergent & Cosmetics , 编辑部邮箱 ,2001年06期
- 【分类号】TQ423.3
- 【被引频次】16
- 【下载频次】359