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气溶胶反应器分解叠氮二乙基铝制备氮化铝纳米粉体
Aerosol Sythesis of Aluminum Nitride Powder Using Diethylaluminun Azide
【摘要】 以叠氮二乙基铝(CH3CH2)2AIN3为前体物在气溶胶反应器中热分解制备氮化铝 AIN纳米粉体.单 反应物且无载气使反应器简化.分解温度低于500-700℃.所得球状AIN纳米粒子平均粒径为10-50 nm,表面积为103m2/g,活性高.该法为AIN 纳米粉体的合成找到了一条新途径.
【Abstract】 A aerosol process is described for making nanometric Aluminum Nitride powder by pyrolysis of single compound Diethylaluminun Azide.The process can produce spherical A1N powder with mean par- ticle diameter ranging from 10 to 50 nm at the temperature of furnace as lower as 500-700. The generated amorpous AIN powder is characterized by a BET surface area of 103m2/g and is very reactive toward moisture. A new way of preparing nanometric powder of AIN is found.
【关键词】 氮化铝;
气溶胶反应器;
纳米粉体;
叠氮二乙基铝;
【Key words】 aluminum nitride; aerosol reactor, nanometric; diethylaluminun azide;
【Key words】 aluminum nitride; aerosol reactor, nanometric; diethylaluminun azide;
- 【文献出处】 北京科技大学学报 ,Journal of University of Science and Technology Beijing , 编辑部邮箱 ,2001年06期
- 【分类号】TB383
- 【被引频次】8
- 【下载频次】145