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β,β’-联萘酚的合成研究
Study on synthesis of 2,2′-dihydroxy-1,1′-dinaphthalene
【摘要】 简要地介绍了β,β′联萘酚的基本性能和用途,对以乙醇为溶剂合成β,β′联萘酚的工艺进行了研究。结果表明最佳的反应条件是n(β萘酚)∶n(FeCl3·6H2O)=1∶2,反应时间为2.5h,反应温度65℃。在此条件下,联萘酚的收率达90%以上。
【Abstract】 The basic properties and applications of 2,2′ dihydroxy 1,1′ dinaphthalene were described compendiously. A synthetic method of 2,2′ dihydroxy 1,1′ dinaphthalene with ethyl alcohol as solvent was studied. The experimental results showed that the optimal reaction conditions were: n (β naphthol)∶ n (FeCl 3·6H 2O)=1∶2,under reaction temperature of 65℃ for 2.5 hours . The yield of the final product was over than 90% with good property.
【关键词】 β,β’-联萘酚;
β萘酚;
手性化合物;
合成;
【Key words】 dihydroxy 1; 1′ dinaphthalene; β naphthol; chiral compound; synthesis;
【Key words】 dihydroxy 1; 1′ dinaphthalene; β naphthol; chiral compound; synthesis;
【基金】 广西青年科学基金!项目 ( No.9815 17)
- 【文献出处】 现代化工 ,MODERN CHEMICAL INDUSTRY , 编辑部邮箱 ,2000年02期
- 【分类号】TQ243.13
- 【被引频次】27
- 【下载频次】621