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反应温度对CVD法批量制备碳纳米管的影响

THEINFLUENCEOF REACTION TEMPERATURE ON THE

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【作者】 肖旭张先锋吴军梁吉徐才录吴德海魏秉庆

【Author】 PREPARATION OF CNTS BY CVD IN LARGE SCALE XIAO Xu, ZHANG Xian-feng, WU Jun, LIANG Ji, XU Cai-lu, WU De-hai, WEI Bing-qing (Department of Mechanical Engineering, Tsinghua University, Beijing 100084,China)

【机构】 清华大学机械工程系!北京100084

【摘要】 用催化裂解法批量制备碳纳米管时,反应温度,反应时间,原料气体流量和催化剂用量等因素对碳纳米管的产量、转化率、微观组织形态有较大影响,其中以反应温度的影响最大。在一定范围内调整裂解温度,可以得到宏观上产量、转化率较高,微观上组织形态较好的碳纳米管。

【Abstract】 All of the experiments involved in this thesis used the method of catalytic pyrolysis of acryl to synthesize Carbon Nanutubes (CNTs). In a stainless steel tube, the reaction room, catalytic pyrolysis of acryl over quartz boats coated uniformly with Ni- Al- diatomite catalyst in the range of 400~ 850 ℃ resulted in the formation of a large number of CNTs which were observed directly by transmission electron microscopy(TEM). The reaction temperature, one of the main factors which affect the productivity of CNTs, is studied systematically. The result of the experiments showed that the reaction temperature had comparatively strong effect on the productivity of CNTs. All the parameters about the reaction temperature indicated above were optimized.

【关键词】 碳纳米管催化裂解法TEM
【Key words】 CNTscatalytic pyrolysis of acrylTEM
  • 【分类号】O613
  • 【被引频次】17
  • 【下载频次】257
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