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高效液相色谱法测定吡虫啉和哒螨灵

Analysis of Imidacloprid and Damanlin by High Performance Liquid Chromatography

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【作者】 何娟常俊标郭瑞云刘澎林素凤陈荣峰王强

【Author】 HE Juan, CHANG Jun-biao, GUO Rui-yun, LIU Peng, LIN Su-feng, CHEN Rong-feng, WANG Qiang (Henan Centre of Analysis and Test, Zhengzhou 450002, China)

【机构】 河南省分析测试中心!河南郑州450002

【摘要】 用高效液相色谱法测定二元混配吡哒可湿性粉剂中的吡虫啉和哒螨灵的质量分数。色谱柱为 μBondapakC1 8柱 (3 .9mm i.d.× 3 0 0 mm) ,流动相为乙腈 -甲醇 -水 (体积比为 60∶ 1 0∶ 3 0 ) ,用二极管阵列检测器 ,检测波长为 2 40 nm,可得到满意的分离效果。

【Abstract】 A new method for determination of imidacloprid and damanlin by using HPLC was established. It was carried out on a μBondapak C18 column (3.9 mm i.d.×300 mm) with ACN\|MeOH\|H\-2O (60∶10∶30,V/V) as eluent and detected at 240 nm using photodiode array detector. The results of imidacloprid and damanlin were 3.71% and 15.65% respectively. The standard deviations for imidacloprid and damanlin were 0.88% and 0.76% respectively.

  • 【文献出处】 色谱 ,CHINESE JOURNAL OF CHROMATOGRAPHY , 编辑部邮箱 ,2000年02期
  • 【分类号】O657.7
  • 【被引频次】11
  • 【下载频次】224
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