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气相色谱分析电合成法制备对氟苯甲醛

GC DETERMINATION OF p-FLUORO-BENZALDEHYDE PREPARED BY ELECTRO-SYNTHESIS

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【作者】 张前前牛淑妍王光信

【Author】 Zhang Qianqian (School of Chemistry and Chemical Engineering, Qingdao University of Oceanography, Qingdao 266003) Niu Shuyan and Wang Guangxin (Dept. of Applied Chemistry, Qingdao Institute of Chemical Engineering)

【机构】 青岛海洋大学化学化工学院!青岛266003青岛化工学院应用化学系

【摘要】 研究了对氟苯甲醛的气相色谱分析条件。选用 8% OV- 2 1 0为固定相测定对氟苯甲醛的含量。方法的标准偏差小于 1 % ,回收率为 1 0 0 .9%~ 1 0 3.3%。方法快速、准确 ,适合于对氟苯甲醛合成工艺中的产品分析

【Abstract】 The optimum analytical conditions for GC determination of p fluorobenzaldehyde is studied and reported in this paper. A stationary phase of 8% OV 210 is chosen for the analysis. Recoveries obtained are in the range of 100.9%~103.3%. RSD′s of this method is found to be less than 1%. The proposed method is rapid and accurate and is suitable to be used in the quality control of the p fluorobenzaldehyde as a product of the electro synthesis

【基金】 山东省科委资助课题
  • 【文献出处】 理化检验(化学分册) ,Physical Testing and Chemical Analysis Partb Chemical Analgsis , 编辑部邮箱 ,2000年12期
  • 【分类号】O657.7
  • 【被引频次】2
  • 【下载频次】99
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