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气相色谱分析电合成法制备对氟苯甲醛
GC DETERMINATION OF p-FLUORO-BENZALDEHYDE PREPARED BY ELECTRO-SYNTHESIS
【摘要】 研究了对氟苯甲醛的气相色谱分析条件。选用 8% OV- 2 1 0为固定相测定对氟苯甲醛的含量。方法的标准偏差小于 1 % ,回收率为 1 0 0 .9%~ 1 0 3.3%。方法快速、准确 ,适合于对氟苯甲醛合成工艺中的产品分析
【Abstract】 The optimum analytical conditions for GC determination of p fluorobenzaldehyde is studied and reported in this paper. A stationary phase of 8% OV 210 is chosen for the analysis. Recoveries obtained are in the range of 100.9%~103.3%. RSD′s of this method is found to be less than 1%. The proposed method is rapid and accurate and is suitable to be used in the quality control of the p fluorobenzaldehyde as a product of the electro synthesis
【基金】 山东省科委资助课题
- 【文献出处】 理化检验(化学分册) ,Physical Testing and Chemical Analysis Partb Chemical Analgsis , 编辑部邮箱 ,2000年12期
- 【分类号】O657.7
- 【被引频次】2
- 【下载频次】99