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含氟苯并咪唑及其衍生物的合成
SYNTHESIS OF BENZOIMINAZOLEFLOURIDE AND ITS DERIVATIVES
【摘要】 合成了四个含氟苯并咪唑衍生物 ,并用红外光谱进行了表征 .探讨了合成该化合物的条件和方法 .结果表明 ,邻苯二胺与芳香酸反应用无水吡啶做溶剂、三氯氧磷作缩合剂以及与醛反应用甲醇作溶剂、铁氰化钾作氧化剂可得较高产率
【Abstract】 Four derivatives of benzominazole containing fluorine were synthesized and the structure determinde by IR spectrum.Research on the synthesis conditions and method showed that products of o-diminebenzene reacting with aromatic acid in dry pyridine solution of POCl 3, reacting with aldehyde in methanol solution of potassium ferricyanide harvested in good yields.
- 【文献出处】 荆州师范学院学报 ,JOURNAL OF JINGZHOU TEACHERS COLLEGE , 编辑部邮箱 ,2000年02期
- 【分类号】O626
- 【被引频次】6
- 【下载频次】239