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火焰原子吸收光谱法测定Mn3O4产品中钙镁含量
Determination of Calcium and Magnesium in Mn3O4 by Flame Atomic Absorption Spectrography
【摘要】 用盐酸加热溶解四氧化三锰样品 ,加入镧盐和锶盐混合释放剂 ,消除 70 %左右基体锰的干扰 ,直接测定其中钙、镁含量 ,样品加标回收率为 96 8%~ 98 2 % ,相对标准偏差为 2 4%~ 3 2 % .
【Abstract】 The sample of Mn 3O 4 is digested with HCl,then La salt and Sr salt are added as release agents to offset 70 percent of influence of matrix Mn,the contents of calcium and magnesium are determined directively which achieve favorable result.This method proved to be convenient,rapid and exact.The recovery of method is 95.8%~98.7% ,the relative standard deviation is 2.43%~3.28%.
【关键词】 四氧化三锰;
混合释放剂;
原子吸收光谱法;
钙;
镁;
【Key words】 Mn 3O 4; compound release agent; Calcium; Magnesium; flame atomic absorption spectrography;
【Key words】 Mn 3O 4; compound release agent; Calcium; Magnesium; flame atomic absorption spectrography;
【基金】 湖南省教委自然科学基金资助项目!(99C6 9)
- 【文献出处】 吉首大学学报(自然科学版) ,JOURNAL OF JISHOU UNIVERSITY(NATURAL SCIENCE EDITION) , 编辑部邮箱 ,2000年01期
- 【分类号】O657.31
- 【被引频次】3
- 【下载频次】113