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SPME—GC—MS联用快速检测赤潮海水中的有机物

RAPID DETECTION OF ORGANIC COMPOUNDS IN SEAWATER DURING REDTIDE BY SPME-GC-MS

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【作者】 赵明桥张展霞李攻科

【Author】 Li Gongke Zhao Mingqiao Zhang Zhanxia(Department of Chemistry , Zhongshan University, Guangzhou, 510275)

【机构】 中山大学化学与化学工程学院!广州510275中山大学化学与化学工程学院!广州510275

【摘要】 本文用固相微萃取(SPME)样品预处理技术,分离富集海水中的有机物,结合气相色谱.质谱(GC-MS)联用技术进行海水中有机物的快速检测.研究了赤潮发生时海水中有机物的种类及含量的变化规律,初步探讨了其变化原因,为研究赤潮的发生机理和赤潮预报提供了科学依据.

【Abstract】 The organic compounds in redtide seawater were detected by solid-phase microextraction (SPME) coupled to gas chromatography mass spectrometry (GC-MS). SPME is a new solventless sample preparation method which could be compatible with high-speed separations. SPME offers a unique combination of sampling (from virtually all matrices) and sample introduction to the GC-MS by means of the same simple device. SPME-GC-MS method is particularly suitable for the detection of organic compounds in seawater matrices. The variations of organic compound concentration and species in redtide seawater were studied in detail. The reason of the variation were discussed briefly. It provided foundation for investigation of redtide mechanism and its prediction.

【关键词】 SPMEGC-MS赤潮海水有机物
【Key words】 SPMEGC-MSredtideseawaterorganic compound.
【基金】 国家自然科学基金资助项目(批准号:29977029)
  • 【文献出处】 环境化学 ,Environmental Chemistry , 编辑部邮箱 ,2000年01期
  • 【分类号】O657.63
  • 【被引频次】18
  • 【下载频次】296
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