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钨硅酸催化合成苯甲酸异戊酯
Catalytic Synthesis of Isoamyl Benzoate with Tungstosilicic Acid
【摘要】 以钨硅酸为催化剂,甲苯为带水剂。苯甲酸和异戊醇,合成苯甲酸异戊酯,酯化率达96.4%。同时,讨论了影响酯化率的各种因素,其最佳反应条件为醇酸物质的量比1.5:1,催化剂用量2.5%,反应时间2.0 h,反应温度120~130℃。
【Abstract】 Isoamyl Benzoate was synthesized with tungstosilicic acid as catalyst and methyl-benzene as water-carrying agent. The optimum raction conditions are alcohol acid mole ratio 1.5:1, catalyst amount 2.5% , reaction time 2.0 h and reaction temperature 120~130℃.The ester yield under this conditions was up to 96.4%.
- 【文献出处】 化工时刊 ,Chemical Industry Times , 编辑部邮箱 ,2000年06期
- 【分类号】TQ655
- 【被引频次】1
- 【下载频次】49