节点文献
5-硝基水杨酸合成工艺的改进
AN IMPROVED TECHNIQUE FOR THE SYNTHESIS OF 5-NITRO-SALICYLIC ACID
【摘要】 用负载型稀土催化剂 ,在无水乙醇介质中 ,用浓硝酸硝化水杨酸 ,使 5 -硝基水杨酸的产率提高到了 80 %以上 ,同时考察了反应温度、反应时间对产率的影响 ,获得了反应的最佳条件
【Abstract】 The nitrification of salicylic acid with nitric acid was studied by using supported rare earth as catalysts and ethanol as solvent.The yield of 5\|nitro\|salicylic acid was raised up to 80%.The influences of temperature and reaction time on the yield of the product were investigated,and the optinum condition was acquired.
【基金】 甘肃省自然科学基金资助项目!( ZR97-0 0 5)
- 【文献出处】 甘肃科学学报 ,JOURNAL OF GANSU SCIENCES , 编辑部邮箱 ,2000年03期
- 【分类号】O625.61
- 【被引频次】8
- 【下载频次】296