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高效液相色谱法测定染色皮革中的致癌芳香胺

Determination of Aromatic Amines in Colored Leather by High Performance Liquid Chromatography

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【作者】 杨燕红梁妙玲肖前

【Author】 Yang Yanhong; Liang Miaoling; Xiao Qian (Guangdong Import & Export commodity Inspection Bureau,China Import & Export Chmmodity Inspection Technology Institute, Guangdong Branch, Guangzhou510623)

【机构】 广东进出口商品检验局中国商检技术研究所广东分所!广州510623

【摘要】 参照德国皮革偶氮染料中间体检测方法,用高效液相色谱法对染色皮革中禁用偶氮染料中间体──18种芳香胺的定性、定量分析进行了研究。结果表明,在一定色谱条件下,除2,4-二氨基苯甲醚和2,4-二氨基甲苯回收率较低外,其它化合物的回收率均达到“DIN53316”方法的要求。

【Abstract】 The qualitative and quantitative analysis of 18 aromatic amines which can be formed through cleavage of banned azo dyes in colored leather were studied hy means of high performance liquid chromtography. The results showed that 18 aromatic amines could be separated effectively under certain chromatographic conditions. The recovery rates for all amines except 2, 4 - diaminoanisole and 2, 4-toluylenediamine were higher much more than the least value required in the method "DIN 53316" .

  • 【文献出处】 分析化学 ,CHINESE JOURNAL OF ANALYTIEAL CHEMISTRY , 编辑部邮箱 ,2000年01期
  • 【分类号】O657.7
  • 【被引频次】17
  • 【下载频次】271
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