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松馏油及其提取物中苯并(a)芘的含量测定

Determination of B(a)p Contents of Pine Tar and Its Extractives

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【作者】 孙晔; 沈海葆; 邱鲁婴;

【Author】 Sun Ye, Shen Haibao, Qiu Laying (Nanjing University of TCM, 210029)

【机构】 南京中医药大学; 南京中医药大学 210029; 210029; 210029;

【摘要】 本文采用纸上层析荧光扫描法测定松馏油及其提取物A、B中苯并(a)芘[B(a)P]的含量。样品经索氏提取器提取后,再以咖啡因-甲酸提取液提取,经乙酰化滤纸纸层析分离,用荧光薄层扫描法测定各样品中B(a)P的含量。结果表明,松馏油及其提取物A、B中B(a)P的含量分别为6171.3、2285.2、129.6ppb,其中以松馏油提取物B中B(a)P的含量最低。

【Abstract】 In this paper, the B(a)P contents of pine tar and its extractives A,B were determined by PC-Scanning method. After combining extraction by caffeine and formic acid with PC-Scanning method, the B(a)P contents were obtained. The results showed the B(a)P contents of pine tar and its extractives A,B were 6171.3 pp,2285.2 ppb,129.6 ppb, among them, the B(a) P content of B was the lowest.

【关键词】 松馏油; 苯并(a)芘;
【Key words】 Pine tar; B(a)P;
  • 【文献出处】 中药材 ,Journal of Chinese Medicinal Materials , 编辑部邮箱 ,1999年05期
  • 【分类号】R284
  • 【被引频次】1
  • 【下载频次】42
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