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车间空气中双乙烯酮的热解吸气相色谱测定方法的研究

Study on Method of the Workplace air-Determination of dikten-Thermal desorption gas Chromatographic

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【作者】 贺宝芝; 刘钢柱; 王淑青; 于海涛; 薛守勇;

【Author】 He Baozhi Liu Gangzhu Wang Shuqing Yu Haitao Xue Shouyong Qingdao Pulic Health and Anti-epidemic Station (266001,China)

【机构】 青岛市卫生防疫站!山东266033;

【摘要】 车间空气中的双乙烯酮采集在硅胶上, 用热解吸经SE- 30 柱分离, 氢焰离子化检测器气相色谱法测定, 方法的检出限为2×10- 3μg。标准曲线线性范围2- 40m g/m 3,解吸效率93.5% ,500m g 硅胶的穿透容量为0.58m g。双乙烯酮样品可保存五天。本方法准确度高、精密度好、快速简便。

【Abstract】 Dikten in air were collected with silicagel with Thermal desorbed and Separted by SE-30 chromatographic column and determined by GC-FID. Detectable limit is 2×10 -3 μg(injection Volume 1ml). The linear range of standard curve was 2-40mg/m 3,and the precision RSD=4.8%-10.1%,and desorbtion efficiency 93.5%. The pass through capacity is 0.58mg Dikten, while the amount of silicegel is 500 mg. The sampling tube be preserved 5 days. This method is rapidity convenience accuracy and reliablity.

  • 【文献出处】 中国卫生检验杂志 ,CHINSES JOURNAL OF HEALTH LABORATORY TECHNOLOGY , 编辑部邮箱 ,1999年06期
  • 【分类号】R134.4
  • 【下载频次】68
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