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罂粟蜂花粉脂肪酸的GC-MS分析

THE ANALYSIS OF FATTY ACID OF BEE POLLEN IN POPPY BY GC-MS

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【作者】 马炳伦李宏

【Author】 MA Binlun, LI Hong (Analysis Testing Centre, Beijing Polytechnical Univ, Beijing 100022, China) (China National Bee Product Quality Supervision Testing Center, Beijing 100073, China)

【机构】 北京工业大学分析测试中心!100022国家蜂产品质量监督检验中心!100073

【Abstract】 The fatty acid of poppy pollen,collected by bee from Gansu, China, has been investigated by GC-MS. We detected about 16 acids in The poppy pollen, including Blltanedioic acid, Octanoic acid, Decanoic acid, Pentadecanoic acid, Hexadecanoic acid, 9,12,15- Octadecatfienoic acid, and Eicosanoic arid. Among Them, Pentadecanoic acid, Decanoic acid, Pentanoic acid Hexadcanoic acid and 9,12,15-Octadecatfienoic acid predominated. Moreover, Different esterfication methods were tried. The best is that in which The sample was extracted by a mixture of Methanol: Cyclohexane: Sulfuric Acid(150:70:75 V/V), partitioned with chloroform and water to separate, dried over Na2SO4, and analysed by GC/MS/DS. About 16 esters were identified. The method is simple and accurate.

【关键词】 Bee-collected pollenpoppyfatty acidGC-MS
【Key words】 Bee-collected pollenpoppyfatty acidGC-MS
  • 【文献出处】 质谱学报 ,JOURNAL OF CHINESE MASS SPECTROMETRY SOCIETY , 编辑部邮箱 ,1999年Z1期
  • 【分类号】O657.63
  • 【下载频次】78
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