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聚花过路黄化学成分的研究
STUDIES ON THE CONSTITUENTS OF LYSIMACHIA CONGESTIFLORA
【摘要】 目的:对聚花过路黄(Lysimachiacongestiflora Hemsl.) 全草的化学成分进行分离和结构鉴定。方法:采用各种色谱技术进行分离,用MS,1HNMR,13CNMR(DEPT) ,1H1HCOSY 谱鉴定化合物。结果:分离得到7 个化合物:杨梅树皮素(1),杨梅树皮苷(2) ,槲皮素(3),柽柳素(4) ,豆甾醇(5) ,仙客来D3OβD吡喃木糖基(1→2)βD吡喃葡糖基(1→4)[βD吡喃葡糖基(1 →2)]αL吡喃阿拉伯糖苷(6) 和珍珠菜苷(7) 。结论:化合物7 为新化合物,化合物4 和6 为首次从珍珠菜属植物中分离得到。
【Abstract】 AIM: To investigate the chemical constituents from Lysimachia congestiflora Hemsl.. METHODS: Column chromatography was used to separate the chemical constituents. MS, IR, 1HNMR , 13 CNMR (DEPT) and 1H 1H COSY were used to determine the structure of the isolated constituents. RESULTS: Seven compounds were identified by spectral analyses as myricetin (1), myricetrin (2), quercetin (3), tamarixetin (4), stigmasterol (5), cyclamiretin D 3 O β D xylopyranosyl (1→2) β D glucopyranosyl (1→4) [β D glucopyranosyl (1→2)] α L arabinopyranoside (6) and lysimachoside (7). CONCLUSION: Compound 7 is a new one. Compounds 4 and 6 were first isolated from the genus of Lysimachia .
- 【文献出处】 药学学报 ,ACTA PHARMACEUTICA SINICA , 编辑部邮箱 ,1999年11期
- 【分类号】R914
- 【被引频次】53
- 【下载频次】281