节点文献
2,6-二烷氧基(羟基)苯乙酮的苄腙和甲腙合成吲唑类化合物
The Synthesis of Indozoles from Substituted Hydranones of 2.6-dialkoxyl (hydroxyl) Acetophenones
【摘要】 在多聚磷酸(PPA)存在下,2,6-二烷氧基(羟基)苯乙酮的苄腙和甲腙可以发生环化反应,生成产率较高的吲唑类化合物。根据实验结果,我们推测反应的关键步骤为亲核进攻。化合物的结构均经元素分析、IR、~1HNMR和MS确定。
【Abstract】 In the presence of PPA ,2.6- dialkoxyl ( hydroxyl) acetophenone hydrazones were cyclized to give indazoles. According to the experimental results, it was assumed that the cyclization was taken by nucleophilic attack. All the new compound were identified by elemental and spectral analyses.
- 【文献出处】 有机化学 ,Chinese Journal of Organic Chemistry , 编辑部邮箱 ,1999年02期
- 【分类号】O626
- 【被引频次】2
- 【下载频次】179