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气相色谱法测定生物制品中苯酚含量
A gas chromatographic method for the determination of phenol content in biologics
【摘要】 本文采用气相色谱法测定了几种生物制品中苯酚含量。样品无需进一步处理,加入内标液后直接上柱测定,色谱峰形良好,线性范围宽,平均回收率和变异系数分别为101.8% 和1.085% ,最小检测限为10 μg/m l,本法操作简单,样品用量少,可作为测定生物制品中苯酚含量的一种常规方法。
【Abstract】 A gas chromatographic method for the determination of phenol in some biologics was developed.The samples added internal standard were chromatographed without further preparation and the chromatopeaks were adequately separated from each other.There was a wide linear relationship of dose response.The average recovery and coefficient of variation were 101.8% and 1.085% respectively.The minimum limitation of detection was 10 μg/ml.The procedure was feasible and simple.So it can be used as the conventional method for assaying phenol in some bioogical products.
- 【文献出处】 微生物学免疫学进展 ,PROGRESS IN MICROBIOLOGY AND IMMUNOLOGY , 编辑部邮箱 ,1999年04期
- 【分类号】R392-33
- 【被引频次】6
- 【下载频次】177