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碳酸锶纳米粉体的制备研究
RESEARCH ON THE SYNTHESIS OF NANOMETER PARTICLE OF STRONTIUM CARBONATE
【摘要】 以分析纯无水硝酸锶和碳酸钠为原料,在旋转填充床中采用液—液相法合成碳酸锶纳米粉体。其条件为:碳酸钠水溶液浓度0.525 m ol/L,硝酸锶水溶液浓度0.5 m ol/L,流量各60 L/h,转速0~1 000 r/m in。得到平均粒径为30 nm 的碳酸锶纳米粉体,粒度分布窄。该法过程简单,产率高,易于工业化。
【Abstract】 Using strontium nitrate(A.R.)and sodium carbonate(A.R.)as raw material,nanometer particles of strontium carbonate were synthesized by mixing the solutions in rotating packed bed.The conditions of the experiment are:the concentration of the solution of sodium carbonate 0.525 mol/L,the concentration of the solution of strontium nitrate 0.5 mol/L,volume of flow 60 L/h respectively,rotating speed 0~1 000 r/min.The average size of the particles is 30~40 nm and the size distribution is very narrow.The process,which has high productivity,is very simple and easy to industrialize.
【Key words】 nanometer particle of strontium carbonate; rotating packed bed; average size;
- 【文献出处】 无机盐工业 ,INORGANIC CHEMICALS INDUSTRY , 编辑部邮箱 ,1999年06期
- 【分类号】TQ132.33
- 【被引频次】28
- 【下载频次】192