节点文献
不同地区高良姜挥发油和1,8-桉油素含量测定比较
Determination of Volatile Oil and 1,8-cineole in Alpinia officinarum Hance from Different Areas by GC
【摘要】 按1995年版《中国药典》方法测定不同地区高良姜的挥发油含量,以及用环己酮作内标、程序升温毛细管气相色谱法测定挥发油中1,8-桉油素的含量。结果显示:不同地区高良姜的挥发油含量各有差异,在0.84%~1.30%之间,其主要成分1,8-桉油素含量为0.268%~0.501%,占挥发油的29.8%~39.8%。1,8-桉油素在2.709~6.574μg的范围内呈线性关系,γ=0.9999,平均回收率为99.3%(n=4,RSD=2.4%)。方法精密度高,重复性好,操作简便。
【Abstract】 The content of volatile oil and 1,8-cineole in Alpinia officinarum Hance from different areas were determined by the methods in the Chinese Pharmacopoeia(1995)and capillary chromatography analysis with cyclohexanone as internal standard respectively.The result:the standard curve of 1,8-cineole was linear in the range of 2.709~6.754 μg, γ=0.9999,average recovery is 99.3%( n=4, RSD=2.4%),the contents of 1,8-cineole and volatile oil are 0.268%~0.501% and 0.84%~1.30% respectively.The method is simple and reliable,and its result is accurate and reproducible.
【Key words】 Alpinia officinarum Hance; Volatile oil; 1,8-cineole; Content determination; GC;
- 【文献出处】 时珍国医国药 ,LiShiZhen Medicine and Materia Medica Research , 编辑部邮箱 ,1999年07期
- 【分类号】R282.710.3,R282.710.
- 【被引频次】7
- 【下载频次】261