【摘要】 以１亚氨基２氰基环戊烷（１Ｉｍｉｎｏ２ｃｙａｎｏｃｙｃｌｏｐｅｎｔａｎｅ简称ＩＣＣＰ）为原料制备环戊醇，工艺过程简单，易于操作，并且使废弃资源得到充分利用．本文讨论脱除ＩＣＣＰ残渣中杂质的方法以及反应中的影响因素．结果表明：酸的加入量对环戊酮收率影响很大，适宜的酸加入量为ＩＣＣＰ的１．４～１．５倍；以骨架镍为催化剂，加氢制环戊醇过程中，当压力一定时，适宜的反应温度为１８０℃左右，适宜的催化剂加入量为原料的３％～４％．更多还原

【Abstract】 The preparation of cyclopentanol from 1 imino 2 cyanocyclopentane, which is a component of the process residue of hexanedinitrile, was investigated. The method of removal of impurity and influencing factors of reactions was discussed. Addition amount of acid has a significant influence on the yield of cyclopentanone, a proper dosage of acid is 140～150 percent of ICCP by weight. In hydrogenation of cyclopentanone, Rany Ni is used as catalyst and its dosage is 3～5 percent of raw material by weight, at pressure of 2～4 MPa, proper reaction temperature is about 180 ℃. Under the above corditions, the yields of cyclopentanone and cyclopentanol were 62 % and 95 % respectively.更多还原