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混合溶剂法测壬基酚聚氧乙烯醚磷酸酯含量
Determination of Contents of Phosphate Polyoxyethylene Nonylphenol by Mixed-Solvents
【摘要】 采用混合溶剂电位滴定法测定壬基酚聚氧乙烯醚磷酸酯中单酯、双酯、磷酸的含量.考察了溶剂种类及其配比,滴定剂溶剂及滴定剂浓度的影响;确定了最佳分析条件:溶剂为95%乙醇/甲苯为1:1;滴定剂为0.2000mol/L标准氢氧化钠乙醇溶液.该方法操作简单、计算方便、可广泛应用于工业生产中.
【Abstract】 The paper shows the content 0f m0no - ester, di - ester and phosphoric acid in phosphateP0lyoxyethylene nonylphenol by mixed - solvents POtentiontric titration. The sort and ratio of the solvents,the solvents and concentrati0ns 0f the titrant were studided. An optimum analytic c0ndition is determined.The alcohol(95 % )/toluene was 1: l; the titrant was 0. 20OO mol. I, - l sodium hydro - xide alcoh0l solution.This method is not only simple in operation but also easy in calculation. lt widely app1ies to industrial pro-duct ion.
【关键词】 混合溶剂法;
壬基酚聚氧乙烯醚磷酸酯;
电位滴定法;
含量;
【Key words】 Mixed-solvent; Phosphate polyoxyethylene nonylphenol; Potentiometric titration; Content;
【Key words】 Mixed-solvent; Phosphate polyoxyethylene nonylphenol; Potentiometric titration; Content;
- 【文献出处】 辽阳石油化工高等专科学校学报 ,JOURNAL OF LIAOYANG PETROCHEMICAL COLLEGE , 编辑部邮箱 ,1999年02期
- 【分类号】O656
- 【被引频次】2
- 【下载频次】95