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亚硫酸氢钠反萃取法提取香兰素工艺特性研究

Study of the Technology Characteristics on Vanillin Extraction with Sodium Bisulfite Solution

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【作者】 苗勇; 亓平言; 雷文; 戴玲妹; 苏玉山;

【Author】 MIAO Yong,QI Ping yan,LEI Wen,DAI Ling mei,SU Yu shan (Department of Chemical Engineering,Tsinghua University,Beijing 100084,China)

【机构】 清华大学化工系!北京100084;

【摘要】 利用特征反应,采用亚硫酸氢钠溶液将香兰素转入水相,再用醋酸丁酯进行二次酸化萃取,从而达到分离提纯香兰素的目的。研究表明,亚硫酸氢钠法提取香兰素的反萃取和酸化萃取过程具有良好的选择性和较高的收率,且酸化萃取受pH和香兰素浓度影响较大,在5gL以下萃取困难。

【Abstract】 According to the characteristic reaction, vanillin could be stripped by the sodium bisulfite solution,then it could be extracted by butyl acetate under acid circumstance,so that vanillin was separated and purified.It was shown that the process of using sodium bisulfite to extract vanillin had high selectivity and yield.The acidifying extraction was influenced deeply by pH value and the concentration of vanillin so it was difficult to extract when the concentration was lower than 5g/L.

【关键词】 香兰素; 亚硫酸氢钠; 萃取; 反萃取;
【Key words】 vanillin; sodium bisulfite; extraction; stripextraction;
  • 【分类号】TQ645
  • 【被引频次】19
  • 【下载频次】307
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