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汽油样品预处理方法的探讨─汽油中痕量铅的测定

The Study of the Pretreatment Method for the Gasoline Samples The Determination of Lead in Gasoline

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【作者】 孙晓娟; 方云如; 张欣; 甘雪; 戴亚锋; 祁建新;

【Author】 Sun Xiaojuan Fang Yunru (Department of Chemical Engineering,Jiangsu Institute of Petrochemical Technology,Changzhou 213016) Qi Jianxin (Kunshan Chemical Group,Kunshan 215300)

【机构】 江苏石油化工学院化学工程系!常州213016; 昆山昆化集团(实业公司)!昆山215300;

【摘要】 研究了测定汽油中痕量铅时两种预处理- 测定方法: (1) 碘- 正辛醇萃取- 硝酸反萃取- 离子交换、洗脱后用阳极溶出法测定; (2) 微波提取- 原子吸收法测定。对两种方法的最佳条件进行了讨论。

【Abstract】 Two kinds of pretreatment method were studied for the determination of trace lead in gasoline:(1)The lead in gasoline was extracted by iodine-1-octanol,reverse-extracted by nitric acid,exchanged by ion exchanger,eluted by hydrochloric acid and determined by Anodic Stripping Voltammetry (ASV).(2)The lead in gasoline was extracted by nitric acid in a WR-1 microwave sample treatment system and then determined by atomic absorption spectrometery(AAS).Some conditions for both method (1) and (2) were optimized.

【关键词】 汽油铅; 预处理; 阳极溶出法; 原子吸收;
【Key words】 Lead gasoline; Pretreatment; ASV; AAS;
【基金】 江苏省自然科学基金
  • 【文献出处】 江苏石油化工学院学报 ,JOURNAL OF JIANGSU INSTITUTE OF PETROCHEMICAL TECHNOLOGY , 编辑部邮箱 ,1999年04期
  • 【分类号】O656.31
  • 【被引频次】2
  • 【下载频次】64
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