节点文献
2,2-二甲基-1,3-丙二醇羟基特戊酸单酯的合成
Synthesis of 2,2-dimethyl-3-hydroxypropyl 2,2-dimethyl-3-hydroxypropanoate
【摘要】 以甲醛、异丁醛为主要原料,开展了2 ,2 - 二甲基- 1 ,3 - 丙二醇羟基特戊酸单酯的小试合成研究,考察了物料配比、温度、反应时间、催化剂用量等因素对反应的影响,产品总收率大于75 % ,纯度99 % 以上。
【Abstract】 Dimethyl-3-hydroxypropyl 2,2-dimethyl-3-hydroxypropanoate was synthesized with formaldehyde and isobutylaldehyde as raw materials. The effects of reactants ratio, temperature, time and catalysts on the reaction were studied. The yield of the product was over 75%. The purity of the product was 99% and over.
【关键词】 甲醛;
异丁醛;
2,2-二甲基-1,3-丙二醇羟基特戊酸单酯;
缩合;
【Key words】 formaldehyde; isobutylaldehyde; 2,2-dimethyl-3-hydroxypropyl 2,2-dimethyl-3-hydroxypropanoate; condensation;
【Key words】 formaldehyde; isobutylaldehyde; 2,2-dimethyl-3-hydroxypropyl 2,2-dimethyl-3-hydroxypropanoate; condensation;
- 【文献出处】 石化技术与应用 ,SCIENCE AND TECHNOLOGY OF LCIC , 编辑部邮箱 ,1999年03期
- 【分类号】TQ224.24
- 【被引频次】2
- 【下载频次】103