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PAN-S分光光度法测定锌的研究
Studying on The PANS Spectrophtometyic Determination of Zinc
【摘要】 研究了用显色剂PAN-S分光光度法测定Zn(Ⅱ)的最佳条件。结果表明:pH值在8.30~10.00范围内Zn(Ⅱ)与PAN-S形成3:1稳定配合物,该配合物的最大吸收波长为535mm,摩尔吸光系数为3.92×104L.cm-1·mol-1;锌量在0~100μg25ml内符合朗伯-比耳定律;加入掩蔽剂可直接测定食品中的锌,回收率为94%~105%。
【Abstract】 It studied that the best conditions for determination of Zinc have at Zinc reacts with PANS to form 3:1 stable complex is at 535nm with molar absorptivity being 3.9210 4 L.cm-1.mol-1. Beer’s Law is obeyed in the range of 0100g Zn()/25ml.THe method has been applied to the direct determination of Zinc in foods with sequestering agents. The recovery is 94%105%.
【基金】 河南教委93916002课题
- 【文献出处】 河南职技师院学报 ,JOURNAL OF HENAN VOCATION-TECHNICAL TEACHERS COLLEGE , 编辑部邮箱 ,1999年02期
- 【分类号】O657.32
- 【被引频次】1
- 【下载频次】148