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强酸型树脂催化L-苯丙氨酸甲酯化研究
STUDY ON METHYL ESTERIFICATION OF L PHENYLALANINE CATALYZED BY STRONG ACID TYPE RESIN
【摘要】 1前言对酯化反应所用催化剂,一般使用强酸,如浓硫酸、浓盐酸等。另外,许多Lewis酸,如三氟化硼、三氯化铝、氯化锌和硅胶等也能促进羰酸提供质子[1]。近年来的研究发现,强酸型阳离子交换树脂亦可用于催化某些酯化过程[2]。L-苯丙氨酸的甲酯化反应,传统...
【Abstract】 The catalytic activity of strong acid type ion exchange resin in esterification of L phenylalanine by methanol was investigated.An optimum technological condition was found as follows, under methanol/L phenylalanine mole ratio 1∶1,catalyst amount 45g/L,temperature 80~85℃ and reaction time 8h.Compared with traditional technology it was an ideal method for producting L phenylalanine methyl ester because of its good yield,low cost and simplicity of operation.
【关键词】 强酸型树脂;
催化剂;
酯化;
L-苯丙氨酸甲酯;
【Key words】 Strong Acid Type Resin; Catalyst; Esterification; L Phenylalanine Methyl Ester;
【Key words】 Strong Acid Type Resin; Catalyst; Esterification; L Phenylalanine Methyl Ester;
- 【文献出处】 化学研究与应用 ,CHEMICAL RESEARCH AND APPLICATION , 编辑部邮箱 ,1999年01期
- 【分类号】O629.711
- 【下载频次】107