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纳米Bi2O3微粒的固相合成及其电化学性能的研究
Solid-phase Synthesis of Nanophase Bi2O3 and Its Electrochemical Properties
【摘要】 用室温和低温固相反应法,采用两种反应途径合成了纳米Bi2O3微粒,并用XRD,TEM,CV及恒流充放实验对其性能进行了研究.
【Abstract】 Nanophase Bi2O3 was synthesized by two methods, treatment of Bi(NO3)3·5H2O with NaOHin solid-state and decomposition of Bi complex prepared by reacting solid Bi(NO3)3·5H2O with 8-OH-quinoline. The crystal form, particle-size , morphology and electrochemical performance of nanophase Bi2O3 were examined with XRD, TEM, CV techniques and charge-discharge experiment. The results indicated that nanophase Bi2O3 exhibited higher electrochemical activities than common-sized Bi2O3.
【关键词】 Bi2O3;
纳米微粒;
固相合成;
电化学性质;
【Key words】 Bi2O3; nanophase particles; solid-phase synthesis; electrochemical properties;
【Key words】 Bi2O3; nanophase particles; solid-phase synthesis; electrochemical properties;
- 【文献出处】 化学学报 ,Acta Chimica Sinica , 编辑部邮箱 ,1999年05期
- 【分类号】TB383
- 【被引频次】88
- 【下载频次】440