节点文献

乙烯酮合成氯乙酰氯的工艺研究

A Technological Study on Synthesis of Chloroacethyl Chloride from Ketene

  • 推荐 CAJ下载
  • PDF下载
  • 不支持迅雷等下载工具,请取消加速工具后下载。

【作者】 李再贵;

【Author】 LI Zaigui (Hunan Research Institute of Chemical Industry Changsha 410007)

【机构】 湖南化工研究院;

【摘要】 介绍了乙烯酮与氯气在溶剂中合成氯乙酰氯的方法。试验了溶剂种类、溶剂用量、反应温度、反应压力的影响。在优惠条件下试验收率达92%以上,产品纯度达985%以上,反应的溶剂回收率达92%以上。

【Abstract】 A method of the synthesis of chloroacethyl chloride from ketene and chlorine in a solvent is introduced. The effects of some conditions, such as the sorts and amounts of solvent, and temperature and pressure of reaction, on the product were studied. The purity of the product and recovery were respectively over 98.5% and 92%, and the recovery of the solvent was up to more than 92%.

  • 【文献出处】 湖南化工 ,HUNAN CHEMICAL INDUSTRY , 编辑部邮箱 ,1999年01期
  • 【分类号】TQ225.3
  • 【被引频次】6
  • 【下载频次】169
节点文献中: 

本文链接的文献网络图示:

本文的引文网络