【摘要】 通过石墨与电解熔盐KF·ZHF所产生的氮气反应，制得了氧化石墨。采用扫描电镜，X射线衍射和红外光谱对其形貌和结构进行测定，并研究了反应温度对氯化石墨结构的影响，初步探讨了氯化石墨的反应机理。更多还原

【Abstract】 Fluoridized graphite was prepared by the reaction of graphite to fluorine gas, which was pro-duced by electrolysis of KF’ 2HF melt salt at l00’C. SEM,XRD and IRS were used to analyze the microstructureof the materials. The effects of the reaction temperature on the microstructure of fluorilized graphite as well as re-acting mechanism were also investigated.更多还原