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HEH[EHP]萃取色层分离-原子发射光谱测定超高纯氧化钬、氧化铒中痕量稀土杂质

Determination of Rare Earth Impurities in Ultra highly Pure Er 2O 3 and Ho 2O 3 by Extraction Chromatography Atomic Emission Spectrometry

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【作者】 李武帅彭春霖袁甫綦文娣高明李丽梅

【Author】 Wushuai LI,Chunlin PENG,Pu YUAN,Wendi QI,Ming GAO and Limei LI Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,130021 Changchun

【机构】 中国科学院长春应用化学研究所

【摘要】 本文研究了2-乙基己基膦酸单2-乙基己酯萃取色层分离-原子发射光谱测定超高纯Ho2O3、Er2O3中良量稀土杂质,可用于99.9999%Ho2O3、Er2O3的纯度分析。

【Abstract】 This article applied (2 ethyhexyldrogen 2 ethylhexyl phosphonate)extraction chromatography to separate 14 rare earth impurities from ultra highly pure Er 2O 3 and Ho 2O 3,and then the impurities were determined by atomic emission spectrometry.The average percentage recovery for each element is in the range of 70%~140%.The relative standard deviations of the determination are ±3 3%~2 2%.This method can be applied to the determination of the trace amounts of rare eath impurities in Er 2O 3 and Ho 2O 3 with a purity of 99 999 9% 99 999 99%.

  • 【文献出处】 光谱学与光谱分析 ,SPECTROSCOPY AND SPECTRAL ANALYSIS , 编辑部邮箱 ,1999年01期
  • 【分类号】O614.33,O657.31
  • 【被引频次】3
  • 【下载频次】65
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