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相转移催化制备α-甲基肉桂醛
The Phase Transfer Catalyzed Synthesis of α Methylcinnaldehyde
【摘要】 首次采用相转移催化剂聚乙二醇(PEG400、PEG600)催化法,合成α甲基肉桂醛新方法,结果表明:PEG400 的催化效果较好,产率达8681% ,比不用催化剂提高近20% 。
【Abstract】 Methylcinnaldehyde was synthesized with phase transfer catalysis polyethylene glycol(PEG).The results showed that the catalytic effect of PEG400 was the best,and the yield reached 86.81%.The purity of α Methylcinnaldehyde was 98.20% by HPLC.The structure of the product was confirmed by IR and MS.The IR spectra was according with ADTLAR standard spectra.
【关键词】 相转移催化;
α-甲基肉桂醛;
聚乙二醇;
合成;
【Key words】 Methylcinnaldehyde; phase transfer catalyst; polyethylene glycol; synthesis;
【Key words】 Methylcinnaldehyde; phase transfer catalyst; polyethylene glycol; synthesis;
- 【文献出处】 日用化学工业 ,CHINA SURFACTANT DETERGENT & COSMETICS , 编辑部邮箱 ,1999年04期
- 【分类号】O625.4
- 【被引频次】8
- 【下载频次】157