【摘要】 硝解 2 ,6,8 ,1 2 四乙酰基 4 ,1 0 二甲酰基六氮杂异伍兹烷 (TAD FIW )制得了 2 ,4 ,6,8,1 0 ,1 2 六硝基六氮杂异伍兹烷 (HNIW ,CL 2 0 ) ,但产物中含有少量副产物。采用柱色谱将其分离 ,经FTIR、1HNMR、MS(CI)及元素分析鉴定 ,证明它为五硝基一甲酰基六氮杂异伍兹烷 (PNMFIW )。更多还原

【Abstract】 Hexanitrohexaazaisowurtzitane(HNIW,CL 20) can be prepared by nitrolysis of 2,6,8,12 tetraacetyl 4,10 diformylhexaazaisowurtzitane(TADFIW). The crude product obtained contains a small amount of impurity. It was separated by column chromatography and identified by FTIR, 1HNMR,MS(CI) and elemental analysis. It is concluded that the impurity is pentanitromonoformylhexaaza isowurtzitane.更多还原